CHE-20057 - Spectroscopy and Analysis
Coordinator: Graeme R Jones Room: LJ1.34 Tel: +44 1782 7 34173
Lecture Time: See Timetable...
Level: Level 5
Credits: 30
Study Hours: 300
School Office: 01782 734921

Programme/Approved Electives for 2020/21

None

Available as a Free Standing Elective

No

Co-requisites

None

Prerequisites

None

Barred Combinations

None

Description for 2020/21

This module is an essential component of the Chemistry and Chemistry with Medicinal Chemistry BSc and MChem programmes at Keele and covers the theory and applications of analytical and spectroscopic techniques including Chromatography, Nuclear Magnetic Resonance, Mass Spectrometry, and large number of related techniques. Laboratory work and data handling exercises build competence at generating and interpreting experimental data, while lectures develop theoretical knowledge. The range of learning activities is designed to continue progress towards the development of Keele's Graduate Attributes with an emphasis on high standards of written communication, and information literacy.

Aims
1.To develop, expand upon and connect fundamental principles of spectroscopy and spectroscopic techniques, and their application to organic and inorganic molecules.
2. To develop understanding of fundamental principles of analytical instrumental techniques and their application in analysis of complex samples.
3. To develop understanding of advanced inorganic chemistry topics such as symmetry and its relationship with structure and spectra.
3. To develop problem-solving skills through data retrieval, generation and analysis.
4. To develop experimental and analytical laboratory skills

Talis Aspire Reading List
Any reading lists will be provided by the start of the course.
http://lists.lib.keele.ac.uk/modules/che-20057/lists

Intended Learning Outcomes

Analyse the symmetry properties of molecules using group theory to predict and relate aspects of molecular structure, bonding and spectra: 1,2
Explain and apply the basic principles of quantitative analysis and data processing and demonstrate an understanding of the context and application of quality assurance in the laboratory: 1,2
Describe and explain the theoretical principles behind a variety of analytical techniques including optical spectroscopy, nuclear magnetic resonance spectroscopy, elemental analysis, chromatography, and mass spectrometry and the reasons for the observed phenomena: 1,2
Critically evaluate the potential of spectroscopic, chromatographic, mass spectrometric, and hyphenated techniques in quantitative analysis: 1,2
1,2
Predict and interpret detailed features of spin-1/2 NMR spectra in organic and inorganic molecules and communicate those interpretations in compliance with standards of presentation in chemistry: 1,2
Analyse and interpret various types of spectral and analytical data obtained from selected techniques (mass spectrometry¿ nuclear magnetic resonance, infrared spectroscopy, elemental analysis) to determine molecular structures: 2
Communicate the analysis, interpretation and significance of experimental results in compliance with scientific writing conventions and standards: 2
Locate, analyse and apply information from literature, chemical databases, and scientific journal articles:

Study hours

Scheduled Learning/Teaching:
Lectures, laboratories, workshops, formative assessments, assessments feedback sessions - 106 hrs
Independent Study:
Independent Study - 194 hrs

School Rules

None

Description of Module Assessment

1: Open Book Assessment weighted 60%
Assessed Problems
A mixture of time limited short and long assessment problems employing a range of question styles and answer formats. The student effort is equivalent to that required to prepare for and complete a 3 hour examination.

2: Portfolio weighted 40%
Coursework Portfolio
A portfolio of laboratory work equivalent to 3500 words (NB: this is a 30-credit module) incorporating data analysis, scientific reporting, professional development and collaborative teamwork